6/7/2003		PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS					samples taken 6/20/01						PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FOREST SOILS
		ENVIRONMENTAL RESPONSE DIVISION					analyzed by 8290 at Triangle Labs
Dioxins/Furans		I SS 1-3			I SS 1-3			6/20/01		I SS 1-3			I SS 1-6			I SS 1-6					I SS 1-6			I SS 1-12			I SS 1-12					I SS 1-12			I SS-2-3				I SS 2-3				I SS 2-3			I SS 2-6								I SS 2-6			I SS 2-12				I SS 2-12				I SS 2-12			I SS 5-3			I SS 5-3					I SS 5-3			I SS 5-6			I SS 5-6					I SS 5-6			I SS 5-12			I SS 5-12					I SS 5-12			I SS 6-3			I SS 6-3					I SS 6-3			I SS 6-6			I SS 6-6					I SS 6-6			I SS 6-12			I SS 6-12					I SS 6-12			I SS 7-3			I SS 7-3					I SS 7-3			I SS 7-6			I SS-7-6					I SS 7-6			I SS 7-12			I SS 7-12					I SS 7-12
		UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL
Analyte in ppt	TEF	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	sampled	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	sampled		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect
	WHO mammal		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero
2378-TCDD	1		2.8						2.8	2.8	2.800	2.800	EMPC,J	0.76					EMPC,J	0.76	0.76	0.76	0.76	EMPC,J	0.23					EMPC,J	0.23	0.23	0.230	0.230		5.9						5.9	5.90	5.90	5.90		3.7						3.7	3.70	3.70	3.70	EMPC,J	0.43					EMPC,J	0.43	0.43	0.43	0.43		7.3						7.3	7.30	7.30	7.30		5.1						5.1	5.10	5.10	5.10	EMPC,J	0.81					EMPC,J	0.81	0.81	0.81	0.81		6.3						6.3	6.3	6.3	6.3		3.4						3.4	3.40	3.40	3.40	ND	0.7					ND	0.7	0.7	0.35	0		5.7						5.7	5.70	5.70	5.70		4.5						4.5	4.50	4.50	4.50	ND	0.3					ND	0.3	0.3	0.15	0
12378-PeCDD	1	J	4.7					J	4.7	4.7	4.700	4.700	J	1.2					J	1.2	1.20	1.20	1.20	ND	0.2					ND	0.2	0.2	0.100	0.000		8						8	8.00	8.00	8.00		7.4						7.4	7.40	7.40	7.40	J	0.76					J	0.76	0.76	0.76	0.76		8.1						8.1	8.10	8.10	8.10		9.1						9.1	9.10	9.10	9.10	J	2.7					J	2.7	2.70	2.70	2.70		7.4						7.4	7.4	7.4	7.4		6.8						6.8	6.80	6.80	6.80	J	1					J	1	1	1	1	EMPC	6.1					EMPC	6.1	6.10	6.10	6.10		12.5						12.5	12.50	12.50	12.50	EMPC,J	0.68					EMPC,J	0.68	0.68	0.68	0.68
123478-HxCDD	0.1	J	3					J	3	0.3	0.300	0.300	EMPC,J	0.71					EMPC,J	0.71	0.07	0.07	0.07	ND	0.2					ND	0.2	0.02	0.010	0.000		4.9						4.9	0.49	0.49	0.49	J	4.1					J	4.1	0.41	0.41	0.41	ND	0.3					ND	0.3	0.03	0.02	0.00	J	4.8					J	4.8	0.48	0.48	0.48		6.5						6.5	0.65	0.65	0.65	J	1.7					J	1.7	0.17	0.17	0.17	J	4.7					J	4.7	0.47	0.47	0.47	J	4.4					J	4.4	0.44	0.44	0.44	ND	0.7					ND	0.7	0.07	0.035	0		4.2						4.2	0.42	0.42	0.42		8.6						8.6	0.86	0.86	0.86	J	0.1					J	0.1	0.01	0.01	0.01
123678-HxCDD	0.1		12.1						12.1	1.21	1.210	1.210	J	2.2					J	2.2	0.22	0.22	0.22	ND	0.2					ND	0.2	0.02	0.010	0.000		23.2						23.2	2.32	2.32	2.32		19.8						19.8	1.98	1.98	1.98	J	1.4					J	1.4	0.14	0.14	0.14		31.5						31.5	3.15	3.15	3.15		26.1						26.1	2.61	2.61	2.61		6.2						6.2	0.62	0.62	0.62		18.5						18.5	1.85	1.85	1.85		17.4						17.4	1.74	1.74	1.74	J	1.3					J	1.3	0.13	0.13	0.13		19.8						19.8	1.98	1.98	1.98		58.6						58.6	5.86	5.86	5.86	ND	0.3					ND	0.3	0.03	0.015	0
123789-HxCDD	0.1		7.2						7.2	0.72	0.720	0.720	J	2.2					J	2.2	0.22	0.22	0.22	ND	0.2					ND	0.2	0.02	0.010	0.000		12.2						12.2	1.22	1.22	1.22		12.7						12.7	1.27	1.27	1.27	J	1.1					J	1.1	0.11	0.11	0.11		13.4						13.4	1.34	1.34	1.34		15.6						15.6	1.56	1.56	1.56	J	4.2					J	4.2	0.42	0.42	0.42		11.3						11.3	1.13	1.13	1.13		11.8						11.8	1.18	1.18	1.18	J	0.92					J	0.92	0.092	0.092	0.092		9.2						9.2	0.92	0.92	0.92		23.7						23.7	2.37	2.37	2.37	ND	0.2					ND	0.2	0.02	0.01	0
1234678-HpCDD	0.01		235						235	2.35	2.350	2.350		35.2						35.2	0.35	0.35	0.35	ND	6.8					ND	6.8	0.068	0.034	0.000		504						504	5.04	5.04	5.04		421						421	4.21	4.21	4.21		28.9						28.9	0.29	0.29	0.29		815						815	8.15	8.15	8.15		460						460	4.60	4.60	4.60		92.4						92.4	0.92	0.92	0.92		385						385	3.85	3.85	3.85		323						323	3.23	3.23	3.23		25.5						25.5	0.255	0.255	0.255		519						519	5.19	5.19	5.19		732						732	7.32	7.32	7.32		20.4						20.4	0.204	0.204	0.204
12346789-OCDD	0.0001		1830						1830	0.183	0.183	0.183		277						277	0.03	0.03	0.03	ND	52.4					ND	52.4	0.00524	0.003	0.000	E	4460			4400			4400	0.44	0.44	0.44		3680						3680	0.37	0.37	0.37		257						257	0.03	0.03	0.03	E	6980			6240			6240	0.62	0.62	0.62	E	4010			3330			3330	0.33	0.33	0.33		845						845	0.08	0.08	0.08	E	4130			3660			3660	0.366	0.366	0.366		3130						3130	0.31	0.31	0.31		234						234	0.0234	0.0234	0.0234	E	4110			2730			2730	0.27	0.27	0.27	E	4430			3280			3280	0.33	0.33	0.33		145						145	0.0145	0.0145	0.0145
2378TCDF	0.1	E	1240			790			790	79	79.000	79.000	EMPC,J	2210			1540			1540	154.00	154.00	154.00		177						177	17.7	17.700	17.700	E	2900			2370			2370	237.00	237.00	237.00	E	1380			938			938	93.80	93.80	93.80	E	983			600			600	60.00	60.00	60.00	E	1290			805			805	80.50	80.50	80.50	E	1620			1140			1140	114.00	114.00	114.00	E	793			517			517	51.70	51.70	51.70	E	14860			1420			1420	142	142	142	E	1870			1410			1410	141.00	141.00	141.00	E	507			377			377	37.7	37.7	37.7	E	1290			915			915	91.50	91.50	91.50	E	1910			1400			1400	140.00	140.00	140.00		189						189	18.9	18.9	18.9
12378-PeCDF	0.05		524						524	26.2	26.200	26.200		762						762	38.10	38.10	38.10		68.7						68.7	3.435	3.435	3.435		835						835	41.75	41.75	41.75		566						566	28.30	28.30	28.30		410						410	20.50	20.50	20.50		514						514	25.70	25.70	25.70		726						726	36.30	36.30	36.30		352						352	17.60	17.60	17.60	EMPC,S,E	2310			675			675	33.75	33.75	33.75		702						702	35.10	35.10	35.10		106						106	5.3	5.3	5.3		671						671	33.55	33.55	33.55		992						992	49.60	49.60	49.60		94.7						94.7	4.735	4.735	4.735
23478-PeCDF	0.5		424						424	212	212.000	212.000		640						640	320.00	320.00	320.00		57.1						57.1	28.55	28.550	28.550		743						743	371.50	371.50	371.50		422						422	211.00	211.00	211.00		308						308	154.00	154.00	154.00		383						383	191.50	191.50	191.50		549						549	274.50	274.50	274.50		264						264	132.00	132.00	132.00	EMPC,S,E	2250			478			478	239	239	239		543						543	271.50	271.50	271.50		113						113	56.5	56.5	56.5		458						458	229.00	229.00	229.00		678						678	339.00	339.00	339.00		67.2						67.2	33.6	33.6	33.6
123478-HxCDF	0.1		377						377	37.7	37.700	37.700		533						533	53.30	53.30	53.30		52.1						52.1	5.21	5.210	5.210		562						562	56.20	56.20	56.20		429						429	42.90	42.90	42.90		282						282	28.20	28.20	28.20		363