06/07/03		PHASE I - SHIAWASSEE WILDLIFE REFUGE - FIELD SOILS							samples taken 5/16/01			PHASE I SHIAWASSEE WILDLIFE REFUGE - FIELD SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FIELD SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FIELD SOILS															PHASE I SHIAWASSEE WILDLIFE REFUGE - FIELD SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FIELD SOILS											PHASE I SHIAWASSEE WILDLIFE REFUGE - FIELD SOILS
		ENVIRONMENTAL RESPONSE DIVISION							analyzed by 8290 at Triangle Labs
Dioxins/Furans		GP 1-6					GP 1-12					GP 2-6			GP 2-6					GP 2-6			GP 2-12			GP 2-12					GP 2-12			GP 3-6					GP 3-12					GP 4-6					GP 4-12			GP 4-12					GP 4-12			GP 5-6			GP 5-6					GP 5-6			GP 5-12			GP 5-12					GP 5-12
		FINAL					FINAL					UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			FINAL					FINAL					FINAL					UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL			UNDILUTED			DILUTED					FINAL
Analyte in ppt	TEF	Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect	Flags	Concentration		Flags	Concentration		Flags	Concentration	nondetect	nondetect	nondetect
	WHO mammal		pg/g	detection level	1/2 d.l.	zero		pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g	detection level	1/2 d.l.	zero		pg/g	detection level	1/2 d.l.	zero		pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero		pg/g			pg/g			pg/g	detection level	1/2 d.l.	zero
2378-TCDD	1	EMPC,B	1.3	1.30	1.30	1.30	B	0.76	0.76	0.76	0.76	B	2.9					B	2.9	2.90	2.90	2.90	B	4.3					B	4.3	4.30	4.30	4.30	B	0.92	0.92	0.92	0.92	B	1.4	1.40	1.40	1.40	J,B	0.47	0.47	0.47	0.47	B	1.3					B	1.3	1.30	1.30	1.30	B	5.9					B	5.9	5.90	5.90	5.90	B	5.5					B	5.5	5.50	5.50	5.50
12378-PeCDD	1	J	0.83	0.83	0.83	0.83	J	0.90	0.90	0.90	0.90	J	1.8					J	1.8	1.80	1.80	1.80		3.4						3.4	3.40	3.40	3.40	EMPC,J	0.82	0.82	0.82	0.82	J	1.2	1.20	1.20	1.20	EMPC,J	0.51	0.51	0.51	0.51	J	2.4					J	2.4	2.40	2.40	2.40	J	1					J	1	1.00	1.00	1.00		3.3						3.3	3.30	3.30	3.30
123478-HxCDD	0.1	J	0.78	0.08	0.08	0.08	J	0.97	0.10	0.10	0.10	EMPC,J	1.4					EMPC,J	1.4	0.14	0.14	0.14	J	2.7					J	2.7	0.27	0.27	0.27	ND	0.30	0.03	0.03	0.03	J	0.88	0.09	0.09	0.09	J,B	0.48	0.05	0.05	0.05	J	2					J	2	0.20	0.20	0.20	EMPC,J	1.1					EMPC,J	1.1	0.11	0.11	0.11	J	3					J	3	0.30	0.30	0.30
123678-HxCDD	0.1	EMPC,J,B	3.8	0.38	0.38	0.38	B	4.00	0.40	0.40	0.40		11.1						11.1	1.11	1.11	1.11		19.2						19.2	1.92	1.92	1.92	EMPC,J,B	2.90	0.29	0.29	0.29	J,B	4.2	0.42	0.42	0.42	J,B	2.1	0.21	0.21	0.21	B	5.1					B	5.1	0.51	0.51	0.51		13.6						13.6	1.36	1.36	1.36		21.4						21.4	2.14	2.14	2.14
123789-HxCDD	0.1	J	2.3	0.23	0.23	0.23	J	2.10	0.21	0.21	0.21	J	4.9					J	4.9	0.49	0.49	0.49		8.3						8.3	0.83	0.83	0.83	J	1.70	0.17	0.17	0.17	J	23	2.30	2.30	2.30	J,B	1.3	0.13	0.13	0.13	J	3.4					J	3.4	0.34	0.34	0.34		10						10	1.00	1.00	1.00		8.7						8.7	0.87	0.87	0.87
1234678-HpCDD	0.01		84	0.84	0.84	0.84		71.50	0.72	0.72	0.72		267						267	2.67	2.67	2.67		328						328	3.28	3.28	3.28		77.10	0.77	0.77	0.77		79.3	0.79	0.79	0.79	B	32.8	0.33	0.33	0.33		54.9						54.9	0.55	0.55	0.55		162						162	1.62	1.62	1.62		400						400	4.00	4.00	4.00
12346789-OCDD	0.0001		735	0.07	0.07	0.07		677.00	0.07	0.07	0.07		2430						2430	0.24	0.24	0.24	E	2630			2800			2800	0.28	0.28	0.28		707.00	0.07	0.07	0.07		741	0.07	0.07	0.07	B	301	0.03	0.03	0.03		532						532	0.05	0.05	0.05		849						849	0.08	0.08	0.08	E	3010			3500			3500	0.35	0.35	0.35
2378TCDF	0.1		104	10.40	10.40	10.40		163.00	16.30	16.30	16.30		397						397	39.70	39.70	39.70	E	1240			1130			1130	113.00	113.00	113.00		175.00	17.50	17.50	17.50		159	15.90	15.90	15.90		95.8	9.58	9.58	9.58		579						579	57.90	57.90	57.90		380						380	38.00	38.00	38.00	E	2810			2920			2920	292.00	292.00	292.00
12378-PeCDF	0.05		47.8	2.39	2.39	2.39		65.40	3.27	3.27	3.27		184						184	9.20	9.20	9.20		346						346	17.30	17.30	17.30		70.20	3.51	3.51	3.51		67.8	3.39	3.39	3.39		44.9	2.25	2.25	2.25		174						174	8.70	8.70	8.70		183						183	9.15	9.15	9.15	EMPC	1530					EMPC	1530	76.50	76.50	76.50
23478-PeCDF	0.5		31	15.50	15.50	15.50		51.00	25.50	25.50	25.50		121						121	60.50	60.50	60.50		331						331	165.50	165.50	165.50		50.90	25.45	25.45	25.45		46.6	23.30	23.30	23.30		30.1	15.05	15.05	15.05		159						159	79.50	79.50	79.50		121						121	60.50	60.50	60.50		941						941	470.50	470.50	470.50
123478-HxCDF	0.1		40.1	4.01	4.01	4.01		59.30	5.93	5.93	5.93		164						164	16.40	16.40	16.40		274						274	27.40	27.40	27.40		59.70	5.97	5.97	5.97		58.7	5.87	5.87	5.87		35.5	3.55	3.55	3.55		143						143	14.30	14.30	14.30		141						141	14.10	14.10	14.10		1240						1240	124.00	124.00	124.00
123678-HxCDF	0.1		9	0.90	0.90	0.90		12.60	1.26	1.26	1.26		31						31	3.10	3.10	3.10		57.8						57.8	5.78	5.78	5.78		12.20	1.22	1.22	1.22		13.1	1.31	1.31	1.31		9	0.90	0.90	0.90		31						31	3.10	3.10	3.10		28.6						28.6	2.86	2.86	2.86		246						246	24.60	24.60	24.60
234678-HxCDF	0.1		6.4	0.64	0.64	0.64		8.50	0.85	0.85	0.85		19.5						19.5	1.95	1.95	1.95		44.1						44.1	4.41	4.41	4.41		8.60	0.86	0.86	0.86		7.9	0.79	0.79	0.79		5.4	0.54	0.54	0.54		18.8						18.8	1.88	1.88	1.88		18.6						18.6	1.86	1.86	1.86		128						128	12.80	12.80	12.80
123789-HxCDF	0.1	J	1.5	0.15	0.15	0.15	J	1.60	0.16	0.16	0.16		3.2						3.2	0.32	0.32	0.32		8.1						8.1	0.81	0.81	0.81	EMPC	1.40	0.14	0.14	0.14	J	1.9	0.19	0.19	0.19	J,B	1.2	0.12	0.12	0.12		5.2						5.2	0.52	0.52	0.52	J	3.5					J	3.5	0.35	0.35	0.35		21						21	2.10	2.10	2.10
1234678-HpCDF	0.01		112	1.12	1.12	1.12		151.00	1.51	1.51	1.51		348						348	3.48	3.48	3.48		588						588	5.88	5.88	5.88		122.00	1.22	1.22	1.22		169	1.69	1.69	1.69		65.8	0.66	0.66	0.66		180						180	1.80	1.80	1.80		167						167	1.67	1.67	1.67		598						598	5.98	5.98	5.98
1234789-HpCDF	0.01	EMPC	5.2	0.05	0.05	0.05		8.00	0.08	0.08	0.08		19.1						19.1	0.19	0.19	0.19		29.4						29.4	0.29	0.29	0.29		7.70	0.08	0.08	0.08		8.1	0.08	0.08	0.08		3.9	0.04	0.04	0.04		10.8						10.8	0.11	0.11	0.11		17.9						17.9	0.18	0.18	0.18		65.7						65.7	0.66	0.66	0.66
12346789-OCDF	0.0001		170	0.02	0.02	0.02		159.00	0.02	0.02	0.02		684						684	0.07	0.07	0.07		612						612	0.06	0.06	0.06		138.00	0.01	0.01	0.01		173	0.02	0.02	0.02		69.7	0.01	0.01	0.01		139						139	0.01	0.01	0.01		257						257	0.03	0.03	0.03		800						800	0.08	0.08	0.08
																																																																											.			.
nondetects = detection limit			TEQ=	38.91				TEQ=	58.03										TEQ=	144.26										TEQ=	354.7				TEQ=	59.03				TEQ=	58.81				TEQ=	34.42										TEQ=	173.17										TEQ=	139.77										TEQ=	1025.68
nondetects = 1/2 d.l.			teq=		38.91			teq=		58.03									teq=		144.26									teq=		354.7			teq=		59.03			teq=		58.81			teq=		34.42									teq=		173.17									teq=		139.77									teq=		1025.68
nondetects = zero			teq=			38.91		teq=			58.03								teq=			144.26								teq=			354.7		teq=			59.03		teq=			58.81		teq=			34.42								teq=			173.17								teq=			139.77								teq=			1025.68
TOTALS		Flags	Concentration	Number			Flags	Concentration	Number			Flags	Concentration	Number	Flags	Concentration	Number	Flags	Concentration	Number			Flags	Concentration	Number	Flags	Concentration	Number	Flags	Concentration	Number			Flags	Concentration	Number			Flags	Concentration	Number			Flags	Concentration	Number			Flags	Concentration	Number	Flags	Concentration	Number	Flags	Concentration	Number			Flags	Concentration	Number	Flags	Concentration	Number	Flags	Concentration	Number			Flags	Concentration	Number	Flags	Concentration	Number	Flags	Concentration	Number
			pg/g					pg/g					pg/g			pg/g			pg/g					pg/g			pg/g			pg/g					pg/g					pg/g					pg/g					pg/g			pg/g			pg/g					pg/g			pg/g			pg/g					pg/g			pg/g			pg/g
TOTAL TCDD			10.1	2				14.8	7				22.1	3					22.1